- #Powder x ray diffraction pro
- #Powder x ray diffraction windows
WinSCP or FileZilla), or a Caltech Box folder.
#Powder x ray diffraction windows
All data is automatically transferred to the XRCF data server which can be accessed as a Windows network drive, SFTP Server (i.e. Data should not be transferred by USB drive from the instrument computer. Those unfamiliar with data analysis procedures but in need of performing such analysis are encouraged to enroll in MS 142. This training is not meant to teach students about the principles of X-ray powder diffraction or data analysis. The focus of this training is on the operation of the instrument. When the training is complete individuals will be able to login to the XRPD reservation site using their Caltech access information and reserve time on the powder diffractometer in 15 min increments. If you are unsure whether instrument training is appropriate contact the director. Contact Michael Takase to schedule a 60 min instrument training session during which we will familiarize you with the collection of X-ray powder diffraction data on either diffractometer. After the safety course, submit a completed New User form. The first step is to take the Caltech EHS X-Ray Diffraction safety course. Staff Assisted Collection (additional fee may apply)Īny samples that will be collected by XRCF staff should be brought to the lab (clearly labeled) along with a completed XRPD Sample Submission Form.Ĭaltech users who will be running more than a few samples are encouraged to complete X-ray safety and instrument training to become independent users. The X-ray powder diffractometers can be run with the assistance of XRCF staff or independently, after training. Both qualitative and quantitative information can be extracted from this diffraction pattern such as the phase composition of the sample, unit cell parameters, crystal size, crystal structure, etc. X-ray powder diffraction is an analytical technique that produces a plot of diffracted X-ray intensity vs the angle of diffraction. #Powder x ray diffraction pro
A Rigaku SmartLab and a Panalytical X'Pert Pro (previously operated by the Faber group and moved from Steele). The XRCF is equipped with two powder diffractometers located in BI 110.
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